Equipment
Technical Infrastructure and Equipment
Electrochemical Equipment
- Various potentiostats for potentiodynamic and potenitostatic EC (Autolab, Bio-logic, Gamry, Jaissle, Solartron, Zennium,…)
- Fast-response & high-frequency pulse potentiostats
- Bipotentiostatic measurements (Autolab)
- Low- and ultra-low current setups for electrochemical single nanoparticle analysis (npi, Elements)
- High current / high potential potentiostats
- Software
- Comsol – finite elements simulations
- DigiElch
- ORCA – DFT simulations
- Electrochemical Quartz Crystal microbalance
- Rotating disc setups (Glassy carbon and Pt electrodes)
- Electrochemical impedance spectroscopy
- Scanning Electrochemical Cell Microscope (probes with microscopic fingerprint)
- Scanning Ion Microscopy
- Scanning Electrochemical Microscope (Au and Pt microelectrodes, 10 um resolution)
- Semiautomatic polishing machine
Surface Characterization
- Scanning Electron microscopy (FEI eSEM Dual Beam™ Quanta 3D FEG), incl. EDX, environmental cell, temperature control
- Atomic Force Microscopy
- JPK Nanowizard, Electrochemical AFM, MFM, conductive-AFM, force-distance measurements
- Bruker Resolve, PeakForce Tapping, Electrochemical AFM, MFM, conductive-AFM, force-distance measurements
- Surface Plasmon-Resonance (Autolab Twingle, standard and EC cuvette)
- Optical microscopy (Zeiss, Axioscope, Bresser)
- Darkfield microscopy
- ATR-SEIRAS spectroelectrochemistry (Veemax III and Jackfish Cell)
- Microscopic FTIR in reflectance/transmission mode
Nanoparticle Characterization
- DLS and Zeta-potential measurements
- Malvern, Zetasizer Nano ZS
- Wyatt, DynaPro NanoStar
- UV-vis spectrometry
- Agilent Cary 60
- Eppendorf BioSpectrometer
- SEM & EDX (FEI, Quanta 3D FEG)
Nanoparticle Synthesis
- 5-port Schlenk lines
- vacuubrand VACUULAN System
- Plasma cleaner
Micro and nano electrode fabrication
- Laser puller (PL-2000 Sutter) for borosilicate and quartz nanopipettes preparation
- Crucible-heated microelectrode sealing (soda lime and borosilicate glass)
- Laser-assisted sealing of metal nanoelectrodes (platinum in quartz)
- Multi-electrode options starting from multi-barrel electrodes
Corrosion Studies
- Büchi Miniclave steel (100bar, 200°C)
- High pressure electrode fitting for the reactor